Grain size analysis plays a pivotal role in geotechnical engineering and construction materials testing. One of the most important procedures used to classify fine-grained soils is the Minus #200 test, also referred to as the wash sieve test. While often overshadowed by full gradation analysis, this simple yet powerful method is essential in understanding the percentage of material finer than the No. 200 (75 µm) sieve.
In this article, we’ll break down the unique procedure, purpose, and interpretation of the Minus #200 test—commonly used across construction sites, soils labs, and quality control operations to support compaction, stability, and site development decisions.
Why the Minus #200 Test Matters
The No. 200 sieve separates silt- and clay-sized particles from sand and gravel. These fine particles significantly influence a soil’s plasticity, drainage characteristics, and load-bearing capacity. Soils with a high percentage of fines can trap moisture, reduce permeability, and lead to soft or unstable conditions under load.
From a construction standpoint, identifying the percentage of fines informs decisions about:
- Soil stabilization methods (e.g., lime or cement treatment)
- Compaction effort required
- Drainage design
- Site work suitability
Materials and Equipment Needed
To ensure accuracy and repeatability, the following items are required:
- #200 (75 μm) standard sieve
- Drying oven (set to 110 ± 5°C)
- Balance readable to 0.01 g
- Wash pan (typically flat-bottomed)
- Graduated cylinder (optional for sedimentation observation)
- Clean water source
- Squeeze bottle and plastic beaker
- Desiccator (optional)
Step-by-Step Minus #200 Test Procedure
This test is typically performed according to ASTM D1140, but labs may adapt procedures based on material type or project-specific requirements. Here is a general procedure tailored for accuracy and clarity:
1. Prepare the Soil Sample for Grain Size Analysis
Obtain a representative soil sample and air dry it, ensuring clumps are gently broken down without crushing aggregate particles. A typical test requires 50 to 100 grams of minus #4 material.
2. Initial Weighing
Record the dry mass of the sample to the nearest 0.01 gram. This value will be used as the baseline for calculating the percentage passing the No. 200 sieve.
3. Wash the Minus #200 Sample
Place the sample in a wash pan. Using clean water, agitate and decant over a No. 200 sieve until the water runs clear. The goal is to remove all particles finer than 75 µm.
Pro tip: Using a squeeze bottle or swirling method ensures fines are effectively washed without excessive water use.
4. Oven Dry the Retained Material
After washing, place the remaining material (from the pan and sieve) in a drying oven at 110 ± 5°C until it reaches a constant mass. This typically takes 12–16 hours.
5. Final Weighing
Once dried, weigh the retained material. The difference between the original mass and the post-wash mass represents the weight of the minus #200 material.
6. Calculations
Use the following formula:
% Finer than No. 200 = [(Initial Mass – Retained Mass) / Initial Mass] × 100
This percentage is reported as the amount of material finer than the #200 sieve.
Interpreting the Minus #200 Results for Grain Size Analysis
A high percentage of minus #200 material often indicates poor drainage, increased plasticity, and a potential for shrink/swell issues. In many specifications, particularly for subgrade or base material, a maximum percentage passing the #200 sieve is strictly defined—typically not exceeding 12–15%.
Exceeding these limits may require:
- Replacing material
- Treating with chemical stabilizers
- Increasing compaction standards
Common Mistakes and Best Practices for Grain Size Analysis
Insufficient Washing: Not thoroughly agitating fines off sand particles leads to under-reporting.
Loss of Sample: Careful handling is essential during decanting to prevent sample loss.
Incomplete Drying: Weighing a damp sample will skew final results.
Inconsistent Sample Size: Ensure test material is representative of field conditions.
When to Use the Minus #200 Test
This test is commonly used in:
- Field quality control for base and subgrade materials
- Borrow pit evaluations
- Stabilization project design
- Soil classification in geotechnical investigations
Final Thoughts for Grain Size Analysis
While simple in execution, the Minus #200 test delivers critical insight into a soil’s engineering behavior. It’s especially useful when full sieve analysis is unnecessary or when verifying compliance with specifications. A well-executed test helps teams avoid costly failures, over-treatment, or project delays caused by unsuitable fines content.
For any contractor, engineer, or lab tech—mastering the minus #200 procedure is a small investment in time with a big return in quality assurance.
Need help with materials testing? Our AASHTO-accredited laboratory specializes in soil classification, compaction testing, and field quality control for public and private projects. Contact us today to learn more.